1: With peracetic acid; acetic acid in water T=-5 - 20°C; 1.5 - 2 h; 2: With palladium dihydroxide in water T=15 - 20°C; 2 h; 3: With hydrogen in water; butan-1-ol T=20 - 25°C; P=2585.81 Torr; 3 h; Product distribution / selectivity;
参考文献
Cox, D. Phillip; Zhang, Yong
Patent: US2008/132703 A1, 2008 ;
Location in patent: Page/Page column 5-6 ;
1: With formic acid; sulfuric acid; dihydrogen peroxide in water T=20°C; 16 h; 2: With 5 palladium on charcoal in water T=20 - 60°C; 20 h; 3: With ammonium hydroxide T=20°C; pH=9.5; 1 h; Overall yield = 2.33 g;
Horsewood, Peter; Kirby, Gordon W.; Sharma, Ram Prakash; Sweeny, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1802 - 1806
in dichloromethane; benzene T=40°C; 4.5 h; Heating; KineticsRate constant;
参考文献
Christie, Clifford C.; Kirby, Gordon W.; McGuigan, Henry; Mackinnon, John W. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2469 - 2474
in benzene Heating; Rate constantMechanismProduct distribution;
参考文献
Kirby, Gordon W.; Sweeny, James G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3250 - 3254
