反应条件
1: 80 percent / pyridinium tosylate / H2O / acetone / 4 h / Heating
2: 1.) n-BuLi / 1.) n-hexane - THF, -70 deg C, 20 min, 2.) 17 h, temperature gradually warmed to room temperature
3: 95 percent / hydrogen / 5percent Pd/C / ethanol / 20 h
View Scheme
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Savchenko, R. G.; Tolstikov, G. A.
Chemistry of Natural Compounds, 1987 , vol. 23, # 4 p. 500 - 502
Khimiya Prirodnykh Soedinenii, 1987 , vol. 23, # 4 p. 595 - 597
