2-氰基-4'-溴甲基联苯合成路线 （共 55 条）
反应条件
N-bromosuccinmide; Azo-bis(2,4-dimethyl-valeronitril) in dichloromethane T=45 - 50°C; 2 - 5 h; Industry scale;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1420016 A1, 2004 ;
Location in patent: Page 16; 17-18 ;
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
参考文献
Sanchez, Ana I.; Martinez-Barrasa, Valentin; Burgos, Carolina; Vaquero, Juan J.; Alvarez-Builla, Julio; Terricabras, Emma; Segarra, Victor
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 8 p. 2370 - 2378
参考文献
Sumika Fine Chemicals Co., Ltd.
Patent: US5621134 A1, 1997 ;
反应条件
N-bromosuccinmide in dichloromethane; water
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5312958 A1, 1994 ;
反应条件
N-bromosuccinmide in tetrachloromethane
参考文献
Sumika Fine Chemicals Co., Ltd.
Patent: US2003/233009 A1, 2003 ;
Location in patent: Page column 8 ;
反应条件
N-bromosuccinmide in tetrachloromethane
反应条件
N-bromosuccinmide in tetrachloromethane
参考文献
US5962500 A1, ;
US 5962500 A
参考文献
US2003/233009 A1, ;
Page column 5 ;
反应条件
1: 71 percent / copper(II) oxide; potassium carbonate; potassium fluoride / palladium(II) bromide; 1,10-phenanthroline / quinoline / 24 h / 170 °C 2: 45 percent / N-bromosuccinimide; azobis(isobutyronitrile) / CCl4; cyclohexane / 18 h / 75 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 19 p. 7473 - 7476
