N-苄氧羰基-L-丙氨酸合成路线 (共 167 条)
反应条件
1: With sodium hydroxide in ethanol; water T=20°C; 0.666667 h; 2: With hydrogenchloride in ethanol; water pH=2;
参考文献
Development Center for Biotechnology
Patent: US2006/287500 A1, 2006 ;
Location in patent: Page/Page column 2; 3 ;
反应条件
sodium carbonate in water T=0 - 20°C; 24 h;
参考文献
Pesic, Alexander; Henkel, Maik; Suessmuth, Roderich D.
Chemical Communications, 2011 , vol. 47, # 26 p. 7401 - 7403
反应条件
morpholine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=30°C; 12 h;
参考文献
Anbazhagan, Mariappan; Reddy, T. Indrasena; Rajappa, Srinivasachari
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 11 p. 1623 - 1627
反应条件
oxygen in acetonitrile 5 h; tyrosinase, phosphate buffer pH 7;
参考文献
Voelkert, Martin; Koul, Surrinder; Mueller, Gernot H.; Lehnig, Manfred; Waldmann, Herbert
Journal of Organic Chemistry, 2002 , vol. 67, # 20 p. 6902 - 6910
反应条件
nitric acid in dichloromethane T=0°C; nitrolysis; 2 h;
参考文献
Strazzolini, Paolo; Scuccato, Massimo; Giumanini, Angelo G.
Tetrahedron, 2000 , vol. 56, # 22 p. 3625 - 3633
反应条件
4-methyl-morpholine in water; acetonitrile T=30°C; P=7500600 Torr; 48 h;
参考文献
Yamamoto, Yoshinori; Furuta, Toshiaki; Matsuo, Jiro; Kurata, Tetsuro
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5737 - 5738
反应条件
α-chymotripsin on Celite; Tris buffer; TEA in acetonitrile T=30°C; 48 h; Yields of byproduct given;
参考文献
Miyazawa, Toshifumi; Tanaka, Kayoko; Ensatsu, Eiichi; Yanagihara, Ryoji; Yamada, Takashi
Tetrahedron Letters, 1998 , vol. 39, # 9 p. 997 - 1000
反应条件
α-chymotripsin on Celite; Tris buffer; TEA in acetonitrile T=30°C; 48 h; Yields of byproduct given;
参考文献
Miyazawa, Toshifumi; Tanaka, Kayoko; Ensatsu, Eiichi; Yanagihara, Ryoji; Yamada, Takashi
Tetrahedron Letters, 1998 , vol. 39, # 9 p. 997 - 1000
反应条件
Ba(ClO4)2; triethylamine in N,N-dimethyl-formamide T=20°C; Substitution; 2 h;
参考文献
Raydnov, M. G.; Klimenko, L. V.; Mitin, Yu. V.
Russian Journal of Bioorganic Chemistry, 1999 , vol. 25, # 5 p. 283 - 287
Bioorganicheskaya Khimiya, 1999 , vol. 25, # 5 p. 323 - 328
反应条件
sulfuric acid; potassium nitrate in dichloromethane T=0°C; 2 h;
参考文献
Strazzolini, Paolo; Giumanini, Angelo G.; Runcio, Antonio
Tetrahedron Letters, 2001 , vol. 42, # 7 p. 1387 - 1389