4,4'-二氯二苯二硫醚合成路线 （共 295 条）
反应条件
hydrogenchloride; potassium hydroxide; dihydrogen peroxide
参考文献
Hiyama, Takehiro; Karino, Hitoshi; Nii, Shinji
Patent: US2003/60665 A1, 2003 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=120°C; 0.0833333 h; microwave irradiation;
参考文献
Ranu, Brindaban C.; Saha, Amit; Jana, Ranjan
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2690 - 2696
反应条件
PPA; potassium iodide in sulfolane T=95 - 100°C; 8 h;
参考文献
Oae; Togo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3813 - 3817
反应条件
samarium diiodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; Reduction; dimerization; 1 h;
参考文献
Byung Woo Yoo; Heung Soo Baek; Sam Rok Keum; Cheol Min Yoon; Ghil Soo Nam; Sung Hoon Kim; Joong Hyup Kim
Synthetic Communications, 2000 , vol. 30, # 23 p. 4317 - 4322
反应条件
hydrogen sulfide in pyridine; acetone
反应条件
hydrazine hydrate in dimethyl sulfoxide T=20°C; 4 h;
参考文献
Zhu, Rui-Heng; Shi, Xiao-Xin
Synthetic Communications, 2012 , vol. 42, # 8 p. 1108 - 1114
反应条件
CuF2; sulfur in dimethyl sulfoxide T=100°C; Chan-Lam Coupling; 12 h; Inert atmosphere;
参考文献
Yu, Jin-Tao; Guo, Huan; Yi, Yuanqiuqiang; Fei, Haiyang; Jiang, Yan
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 749 - 752
反应条件
zinc in benzene T=6 - 8°C; 16 h;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 35, p. 375 - 386
反应条件
(2,2,4,4-tetrafluoropropoxy)tellurane in diethyl ether T=-50 - -40°C; 0.166667 h;
参考文献
Stukalo, E. A.; Yur'eva, E. M.; Markovskii, L. N.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 301 - 303
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 2 p. 343 - 346
反应条件
sulfur; potassium fluoride in water; N,N-dimethyl-formamide T=150°C; 0.42 h;
参考文献
Gingras, Marc; Chabre, Yoann M.; Raimundo, Jean-Manuel
Synthesis, 2004 , # 12 p. 2052 - 2057
