4,4'-二氯二苯二硫醚合成路线 （共 295 条）
反应条件
1: With isopropylmagnesium chloride in tetrahydrofuran T=-20°C; 0.5 h; 2: With zinc dibromide in tetrahydrofuran T=-40°C; 0.5 h; 3: With disulfur dichloride in tetrahydrofuran
参考文献
Korn, Tobias J.; Knochel, Paul
Synlett, 2005 , # 7 art. no. G06105ST, p. 1185 - 1187
反应条件
di-p-methoxyphenyl telluride; 5,15,10,20-tetraphenylporphyrin in dichloromethane T=0°C; 0.25 h; Irradiation;
参考文献
Oba, Makoto; Tanaka, Kazuhito; Nishiyama, Kozaburo; Ando, Wataru
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 4173 - 4177
反应条件
samarium; titanium tetrachloride in tetrahydrofuran T=60°C; 2 h;
参考文献
Wang; Zhang
Synthetic Communications, 1996 , vol. 26, # 1 p. 135 - 138
反应条件
trimethylsilyl iodide in dichloromethane 16 h; Ambient temperature;
参考文献
Olah, George A.; Narang, Subhash C.; Field, Leslie D.; Salem, George F.
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4792 - 4793
反应条件
dihydrogen peroxide in methanol; water
参考文献
Sumitomo Seika Chemicals Co., Ltd.
Patent: US5741933 A1, 1998 ;
反应条件
dihydrogen peroxide; chlorine in methanol; water
参考文献
Sumitomo Seika Chemicals Co., Ltd.
Patent: US5741933 A1, 1998 ;
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in N,N-dimethyl acetamide T=20°C; P=760.051 Torr; 6 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 53, # 43 p. 5729 - 5732
反应条件
titanium(IV) isopropylate; carbon monoxide; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=150 - 160°C; P=7600 Torr;
参考文献
Chemistry Letters, , p. 77 - 78
反应条件
1: With magnesium in tetrahydrofuran T=25°C; 10 h; 2: With zinc dibromide in tetrahydrofuran T=-40°C; 0.5 h; 3: With disulfur dichloride in tetrahydrofuran
参考文献
Korn, Tobias J.; Knochel, Paul
Synlett, 2005 , # 7 art. no. G06105ST, p. 1185 - 1187
反应条件
tetra-n-butylammonium perchlorate in carbon disulfide; ethanol T=0°C; Electrochemical reaction;
参考文献
Barba, Fructuoso; Ranz, Fernando; Batanero, Belen
Tetrahedron Letters, 2009 , vol. 50, # 49 p. 6798 - 6799
