1-(1,2,3,4-四氢喹啉-6-基)乙酮合成路线 (共 11 条)
反应条件
hydrogenchloride; aluminium trichloride 1) CS2, reflux, 8 h, 2) reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gruenenthal GmbH
Patent: US2010/234340 A1, 2010 ;
Location in patent: Page/Page column 22 ;
US 20100234340 A1
反应条件
hydrogenchloride; water; iron Reagens 4: Aethanol;
参考文献
de Diesbach et al.
Helvetica Chimica Acta, 1952 , vol. 35, p. 2322,2330
反应条件
hydrogenchloride; aluminium trichloride 1) CS2, CH2ClCH2Cl, reflux, 8 h, 2) reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ishihara, Yuji; Tanaka, Toshimasa; Goto, Giichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3401 - 3406
反应条件
hydrogenchloride; aluminium trichloride 1) CS2, reflux, 8 h, 2) reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ishihara, Yuji; Tanaka, Toshimasa; Goto, Giichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3401 - 3406
反应条件
hydrogenchloride; aluminium trichloride 1) CS2, reflux, 8 h, 2) reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ishihara, Yuji; Tanaka, Toshimasa; Goto, Giichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3401 - 3406
反应条件
hydrogenchloride; aluminium trichloride 1) CS2, reflux, 8 h, 2) reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ishihara, Yuji; Tanaka, Toshimasa; Goto, Giichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3401 - 3406
反应条件
hydrogenchloride; aluminium trichloride 1) CS2, reflux, 8 h, 2) reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ishihara, Yuji; Tanaka, Toshimasa; Goto, Giichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3401 - 3406
反应条件
hydrogenchloride; aluminium trichloride 1) CS2, reflux, 8 h, 2) reflux, 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ishihara, Yuji; Tanaka, Toshimasa; Goto, Giichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3401 - 3406
反应条件
hydrogenchloride; aluminium trichloride multistep reaction; other NH protective groups; other N-heterocycles; influence of the N-protective groups and of ring size on the ratio of regioisomers;
参考文献
Ishihara, Yuji; Tanaka, Toshimasa; Goto, Giichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3401 - 3406
反应条件
dihydrogen peroxide; sodium tungstate in methanol 24 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, # 6 p. 1744 - 1749