1,1-环己基二甲酸乙酯合成路线 （共 29 条）
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 7 p. 2266 - 2267
参考文献
Zhurnal Obshchei Khimii, , vol. 22, p. 1944,1951; engl. Ausg. S. 1993, 1998, 1999
参考文献
Zhurnal Obshchei Khimii, , vol. 22, p. 1944,1951; engl. Ausg. S. 1993, 1998, 1999
参考文献
Journal of the American Chemical Society, , vol. 43, p. 1368
反应条件
potassium hydroxide; 18-crown-6 ether in ethanol; benzene 1.) room temperature, 3 h, 2.) reflux, 22 h;
参考文献
Hunter, Duncan H.; Patel, Vijay; Perry, Richard A.
Canadian Journal of Chemistry, 1980 , vol. 58, # 21 p. 2271 - 2277
反应条件
1: 89 percent / NaAlH2(OCH2OCH3)2 / tetrahydrofuran 2: 68 percent / pyridine 3: 72 percent / LiBr / 2-ethoxy-ethanol 4: 75 percent / Zn, ethylenediaminetetraacetic acid tetrasodium salt / ethanol View Scheme
参考文献
Fajgar, Radek; Pola, Josef
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7709 - 7717
反应条件
1: 89 percent / NaAlH2(OCH2OCH3)2 / tetrahydrofuran 2: 68 percent / pyridine 3: 72 percent / LiBr / 2-ethoxy-ethanol View Scheme
参考文献
Fajgar, Radek; Pola, Josef
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7709 - 7717
反应条件
lithium aluminium tetrahydride
参考文献
Fajgar, Radek; Pola, Josef
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7709 - 7717
反应条件
1: NaOH; H2O / 48 h / 20 °C 2: 56 percent / SF4 / 3 h / 30 °C 3: 88 percent / NaOH; H2O; Bu4NHSO4 / dimethylsulfoxide / 48 h / 20 °C View Scheme
参考文献
Dmowski, Wojciech; Wolniewicz, Adam
Journal of Fluorine Chemistry, 2000 , vol. 102, # 1-2 p. 141 - 146
反应条件
1: NaOH; H2O / 48 h / 20 °C 2: 56 percent / SF4 / 3 h / 30 °C View Scheme
参考文献
Dmowski, Wojciech; Wolniewicz, Adam
Journal of Fluorine Chemistry, 2000 , vol. 102, # 1-2 p. 141 - 146
