1: With triethylamine in N,N-dimethyl-formamide; toluene Curtius rearrangement; 3 h; Heating; 2: With potassium hydroxide; glycerol in ethanol; N,N-dimethyl-formamide; toluene 2 h; Heating; Further stages.;
参考文献
European Journal of Organic Chemistry, , # 2 p. 337 - 342
tris-(dibenzylideneacetone)dipalladium(0); sodium hydroxide; di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine in 1,4-dioxane; polyethylene glycol; water T=80°C;
参考文献
Journal of Physical Chemistry A, , vol. 114, # 11 p. 3932 - 3938
