N,N-二甲基-4-联苯胺合成路线 （共 82 条）
反应条件
Pd2(p-tolyl)2(.mu.-I)(.mu.-N,N'-bis[2-(diphenylphosphino)phenyl]formamidinato); potassium carbonate in benzene
T=100°C; Suzuki-Miyaura Coupling; 17 h; Overall yield = 40 percent;
参考文献
Tsukada, Naofumi; Abe, Tsubasa; Inoue, Yoshio
Helvetica Chimica Acta, 2013 , vol. 96, # 6 p. 1093 - 1102
反应条件
in acetonitrile
T=20°C; 0.166667 h; Irradiation;
参考文献
Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1282 - 1289
反应条件
[Ni0(1,5-cyclooctadiene)2]; zirconium (IV) fluoride; cesium fluoride; tri-cyclo-hexyl-phosphine in toluene
T=20 - 100°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Xu, Tian; Shimasaki, Toshiaki; Chatani, Naoto
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19505 - 19511
反应条件
[Ni0(1,5-cyclooctadiene)2]; cesium fluoride; tri-cyclo-hexyl-phosphine in toluene
T=20 - 100°C; Suzuki-Miyaura coupling; 2 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Xu, Tian; Shimasaki, Toshiaki; Chatani, Naoto
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19505 - 19511
反应条件
[Ni0(1,5-cyclooctadiene)2]; cesium fluoride; tri-cyclo-hexyl-phosphine in toluene
T=20 - 100°C; Suzuki-Miyaura coupling; 2 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Xu, Tian; Shimasaki, Toshiaki; Chatani, Naoto
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19505 - 19511
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [Ni0(1,5-cyclooctadiene)2]; cesium fluoride in toluene
T=20 - 100°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Xu, Tian; Shimasaki, Toshiaki; Chatani, Naoto
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19505 - 19511
反应条件
sodium tetrahydroborate
T=150 - 250°C;
参考文献
Yang, Cangming; Pittman Jr., Charles U.
Tetrahedron Letters, 1997 , vol. 38, # 37 p. 6561 - 6564
反应条件
in acetonitrile
Irradiation;
参考文献
Fagnoni, Maurizio; Mella, Mariella; Albini, Angelo
Organic Letters, 1999 , vol. 1, # 8 p. 1299 - 1301
反应条件
triethylamine in acetonitrile
16 h; Irradiation;
参考文献
Dichiarante, Valentina; Betti, Cecilia; Fagnoni, Maurizio; Maia, Angelamaria; Landini, Dario; Albini, Angelo
Chemistry - A European Journal, 2007 , vol. 13, # 6 p. 1834 - 1841
反应条件
PhOSO2CF2CF2OCF2CF2H
21 h; Irradiationfurther aryl perfluoroalkanesulfonates as reagents; Further byproducts given;
参考文献
Chen, Qing-Yun; Li, Zhan-Ting
Journal of Fluorine Chemistry, 1994 , vol. 66, # 1 p. 59 - 62
