N,N-二甲基-4-联苯胺合成路线 （共 82 条）
反应条件
Ni(PCy3)2Cl2; tri-cyclo-hexyl-phosphine in various solvent(s)
T=70°C; 15 h;
参考文献
Dankwardt, John W.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 18 p. 2428 - 2432
反应条件
stilbazo; palladium diacetate; potassium carbonate in water
T=20°C; Suzuki-Miyaura cross-coupling reaction; Inert atmosphere;
参考文献
Peng, Yi-Yuan; Liu, Jinbiao; Lei, Xiaoli; Yin, Zenlan
Green Chemistry, 2010 , vol. 12, # 6 p. 1072 - 1075
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4901 - 4904
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4901 - 4904
反应条件
catalyst 1 (aliphatic, phosphine based pincer complex of palladium) in 1,4-dioxane; 1-methyl-pyrrolidin-2-one
T=100°C; Negishi cross-coupling reaction; 0.3 h;
参考文献
Gerber, Roman; Blacque, Olivier; Frech, Christian M.
Dalton Transactions, 2011 , vol. 40, # 48 p. 12939 - 12941
反应条件
triphenyl phosphite; K3PO4*3H2O; Ipr.HCl; palladium diacetate in tert-butyl alcohol
T=80°C; 10 h; Inert atmosphere;
参考文献
Chen, Xiaofeng; Ke, Haihua; Chen, Yao; Guan, Changwei; Zou, Gang
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7572 - 7578
反应条件
C35H31BrN4NiP in tetrahydrofuran
T=25°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1054 - 1061
反应条件
potassium carbonate in tetrahydrofuran; water
24 h;
参考文献
Matter, Hans; Schudok, Manfred; Schwab, Wilfried; Thorwart, Werner; Barbier, Denis; Billen, Guenter; Haase, Burkhard; Neises, Bernhard; Weithmann, Klaus-Ulrich; Wollmann, Theo
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 11 p. 3529 - 3544
反应条件
xanthone powder in acetonitrile
T=20°C; Photolysis;
参考文献
Milanesi, Silvia; Fagnoni, Maurizio; Albini, Angeld
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 603 - 610
反应条件
C68H72Cl2N6NiP2 in toluene
T=120°C; 16 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2011 , vol. 17, # 18 p. 4972 - 4975
