2-(2-吡啶)-苯并咪唑合成路线 (共 19 条)
反应条件
(NH4)2S2O8; sodium lauryl sulfate in water T=25°C; 0.166667 h; Micellar solution;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Nejati, Akbar
Green Chemistry, 2010 , vol. 12, # 7 p. 1237 - 1241
反应条件
polyphposphoric acid T=180°C; 2 h;
参考文献
Schiffmann, Rolf; Neugebauer, Alexander; Klein, Christian D.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 2 p. 511 - 522
反应条件
sulfur in neat (no solvent) T=110°C; 16 h; Inert atmosphere;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Dean, William A.; Al-Mourabit, Ali
Organic Letters, 2012 , vol. 14, # 23 p. 5948 - 5951
反应条件
sodium hydroxide; PPA in dichloromethane; acetic acid
参考文献
Ott, Gregory R.; Chen, Xiao-Tao; Duan, Jingwu; Lu, Zhonghui
Patent: US2003/139388 A1, 2003 ;
反应条件
sulfur in neat (no solvent) T=110°C; 16 h; Inert atmosphere;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Dean, William A.; Al-Mourabit, Ali
Organic Letters, 2012 , vol. 14, # 23 p. 5948 - 5951
反应条件
[Fe(phthalocyanine)]; sodium t-butanolate in toluene T=120°C; 36 h; Inert atmosphere;
参考文献
Bala, Manju; Verma, Praveen Kumar; Sharma, Upendra; Kumar, Neeraj; Singh, Bikram
Green Chemistry, 2013 , vol. 15, # 6 p. 1687 - 1693
反应条件
sulfur T=160 - 170°C; 10 h;
参考文献
Hisano; Ichikawa; Tsumoto; Tasaki
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 8 p. 2996 - 3004
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane Heating;
参考文献
Tandon, Vishnu K.; Kumar, Manoj
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 4185 - 4187
反应条件
1: 1,2-diamino-benzene With diethylaluminium chloride in toluene T=0 - 20°C; 2: hydroxymethyl JandaJelTM resin-bound 2-pyridyl ester in toluene 24 h; Heating; Further stages.;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
sodium sulfide; sulfur T=160 - 170°C; 15 h;
参考文献
Yutilov, Yu. M.; Shcherbina, L. I.; Smolyar, N. N.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 3.2 p. 461 - 463
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 3 p. 429 - 430