反应条件
magnesium in diethyl ether 1.) reflux, 4.5 h, 2.) -60 - -45 deg C, 1 h; room temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Duncan, James A.; Bohle, D. Scott; Blanchard, Charles A.; Bosse, Mark L.; Noland, Terry W.; et al.
Journal of the American Chemical Society, 1982 , vol. 104, # 10 p. 2837 - 2839