3-苄基-2,4-戊二酮合成路线 (共 48 条)
反应条件
carbon monoxide; hydrogen; tri-ruthenium(0)dodecacarbonyl in N,N-dimethyl-formamide
T=150°C; P=76000.1 Torr; 16 h;
参考文献
Abe, Fujio; Hayashi, Teruyuki; Tanaka, Masato
Chemistry Letters, 1990 , # 5 p. 765 - 768
反应条件
aluminum oxide; potassium tert-butylate
4 h;
参考文献
Ranu, Brindaban C.; Bhar, Sanjay
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 3 p. 365 - 368
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; water
T=23°C;
参考文献
Christoffers, Jens
Synthetic Communications, 1999 , vol. 29, # 1 p. 117 - 122
反应条件
sodium in acetonitrile
T=40°C; 12 h;
参考文献
Yoshihara, Nobutoshi; Kitagawa, Teruhiro; Ihara, Ikuko; Hasegawa, Sadao; Hasegawa, Tadashi
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 4 p. 1185 - 1187
反应条件
in chloroform
T=120°C; 0.25 h;
参考文献
Marquet, J.; Moreno-Manas, M.; Pacheco, P.; Vallribera, A.
Tetrahedron Letters, 1988 , vol. 29, # 12 p. 1465 - 1468
反应条件
3 A molecular sieve; piperidinium acetate; potassium carbonate; 1,1'-bis-(diphenylphosphino)ferrocene; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in toluene
T=110°C; Knoevenagel reaction; 24 h;
参考文献
Black, Phillip. J.; Cami-Kobeci, Gerta; Edwards, Michael G.; Slatford, Paul A.; Whittlesey, Michael K.; Williams, Jonathan M. J.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 1 p. 116 - 125
反应条件
sodium hydride in tetrahydrofuran
T=0 - 20°C;
参考文献
Nakano, Takeo; Endo, Kohei; Ukaji, Yutaka
Organic Letters, 2014 , vol. 16, # 5 p. 1418 - 1421
参考文献
House; Gannon
Journal of Organic Chemistry, 1958 , vol. 23, p. 879,882
反应条件
bis(acetylacetonato) palladium; triphenylphosphine in acetylacetone
T=140°C; 24 h;
参考文献
Moreno-Manas, M.; Trius, A.
Tetrahedron, 1981 , vol. 37, # 17 p. 3009 - 3016
参考文献
Sprague; Beckham; Adkins
Journal of the American Chemical Society, 1934 , vol. 56, p. 2665,2666