4,4'-二甲基-2,2'-联吡啶合成路线 （共 79 条）
反应条件
T=21.85°C; Equilibrium constant;
参考文献
Nabavizadeh, S. Masoud
Dalton Transactions, 2005 , # 9 p. 1644 - 1648
反应条件
1: With tert-butoxy-bis-(dimethylamino)methane in N,N-dimethyl-formamide T=140°C; 2: With sodium periodate in tetrahydrofuran; water T=20°C; Further stages.;
参考文献
Viau, Lydie; Senechal, Katell; Maury, Olivier; Guegan, Jean-Paul; Dupau, Philippe; Toupet, Loic; Le Bozec, Hubert
Synthesis, 2003 , # 4 p. 577 - 583
反应条件
1: With selenium(IV) oxide in 1,4-dioxane 24 h; Reflux; 2: With sodium tetrahydroborate in methanol T=20°C; 1 h;
参考文献
Li, Minna; Liang, Qichao; Zheng, Meiqing; Fang, Chenjie; Peng, Shiqi; Zhao, Ming
Dalton Transactions, 2013 , vol. 42, # 37 p. 13509 - 13515
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 3 h; Heating;
参考文献
Hirata, Narukuni; Lagref, Jean-Jacques; Palomares, Emilio J.; Durrant, James R.; Nazeeruddin, M. Khaja; Gratzel, Michael; Di Censo, Davide
Chemistry - A European Journal, 2004 , vol. 10, # 3 p. 595 - 602
反应条件
chromium(VI) oxide; sulfuric acid
参考文献
Bakhtchadjian, Robert; Tsarukyan, Samvel; Barrault, Joel; Martinez, Fernando O.; Tavadyan, Levon; Castellanos, Nelson J.
Transition Metal Chemistry, 2011 , vol. 36, # 8 p. 897 - 900
反应条件
potassium permanganate; sulfuric acid 12 h; Heating;
参考文献
Australian Journal of Chemistry, , vol. 39, # 7 p. 1053 - 1062
反应条件
1: oxidation 3: ammonia 4: 88 percent / trichlorooxophosphorus / 61 h / ultrasonication View Scheme
参考文献
Baxter, Paul N.W.; Connor, Joseph A.
Journal of Organometallic Chemistry, 1988 , vol. 355, p. 193 - 196
反应条件
1: 50 percent / aq. H2SO4; KMnO4 / 12 h / Heating 2: 99 percent / conc. H2SO4 / 60 h / Heating View Scheme
参考文献
Luetzen, Arne; Hass, Oliver; Bruhn, Torsten
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1807 - 1811
反应条件
1: 4,4'-dimethyl-2,2'-bipyridine With chromium(VI) oxide; sulfuric acid T=0 - 80°C; 2: methanol With sulfuric acid Reflux;
参考文献
Ohkanda, Junko; Satoh, Ritsuko; Kato, Nobuo
Chemical Communications, 2009 , # 45 p. 6949 - 6951
反应条件
1: 50 percent / aq. H2SO4; KMnO4 / 12 h / Heating 2: 99 percent / conc. H2SO4 / 60 h / Heating 3: 30 percent / NaBH4 / methanol / 60 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 18 p. 5919 - 5925
