2,3,4,5-四氯-6-(三氯甲基)吡啶合成路线 （共 15 条）
反应条件
chlorine in tetrachloromethane 1 h; HeatingIrradiation;
参考文献
Journal of Organic Chemistry, , vol. 53, # 6 p. 1267 - 1273
参考文献
Kalama Chemical, Inc.
Patent: US4517369 A1, 1985 ;
反应条件
chlorine in tetrachloromethane 0.5 h; HeatingIrradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 5 p. 1101 - 1105
反应条件
chlorine T=200°C; 18 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 6 p. 1168 - 1171
Zhurnal Organicheskoi Khimii, , vol. 19, # 6 p. 1308 - 1312
反应条件
sodium hydroxide 2 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 45, # 5 p. 1079 - 1085
反应条件
ammonia T=100°C; 1 h;
参考文献
Ovchinnikov, V.G.; Nasyr, I.A.; Litvinenko, G.S.; Maksimeno, N.M.; Zatsarevnyi, V.M.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 12 p. 2490 - 2497,2327 - 2334
反应条件
ammonia T=100°C; 1 h;
参考文献
Ovchinnikov, V.G.; Nasyr, I.A.; Litvinenko, G.S.; Maksimeno, N.M.; Zatsarevnyi, V.M.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 12 p. 2490 - 2497,2327 - 2334
反应条件
1: 1.1 percent Chromat. / NH3 / 1 h / 100 °C 2: 97.1 percent / NH3 / dimethylsulfoxide / 22 h / 100 °C View Scheme
参考文献
Ovchinnikov, V.G.; Nasyr, I.A.; Litvinenko, G.S.; Maksimeno, N.M.; Zatsarevnyi, V.M.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 12 p. 2490 - 2497,2327 - 2334
反应条件
1: 60.2 percent / NaOH / 2 h / Heating 2: 97 percent / AlCl3 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Tiwari, Anita; Riordan, James M.; Waud, William R.; Struck, Robert F.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 5 p. 1079 - 1085
反应条件
chlorine T=200°C; Rate constant;
参考文献
Emel'yanov, V. I.; Stul', B. Ya.; Korolev, B. M.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 6 p. 1168 - 1171
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 6 p. 1308 - 1312
