2-羟基亚氨基对甲苯乙酰胺合成路线 （共 12 条）
反应条件
hydrogenchloride; hydroxylamine hydrochloride; water; sodium sulfate Reflux;
参考文献
Wang, Lihong; Li, Zhanshan; Lu, Lianhong; Zhang, Wei
Tetrahedron, 2012 , vol. 68, # 5 p. 1483 - 1491
反应条件
hydroxylammonium sulphate; sodium sulfate in water T=60 - 80°C; 2 h;
参考文献
Garden, Simon J.; Torres, Jose C.; Ferreira, Alexandre A.; Silva, Rosangela B.; Pinto, Angelo C.
Tetrahedron Letters, 1997 , vol. 38, # 9 p. 1501 - 1504
反应条件
hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate in ethanol; water T=80°C; 3 h;
参考文献
Krapcho, A. Paul; Cadamuro, Sergio A.
Organic Preparations and Procedures International, 2004 , vol. 36, # 1 p. 74 - 76
反应条件
hydroxylamine hydrochloride; sodium sulfate in water 10 h; Heating;
参考文献
Gupta, Neeti; Singh
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 1998 , vol. 37, # 1 p. 75 - 79
反应条件
hydroxylamine hydrochloride
参考文献
Thota, Sreekanth; Karki, Subhas Somalingappa; Jayaveera; Balzarini, Jan; Clercq, Erik De
Journal of Coordination Chemistry, 2010 , vol. 63, # 24 p. 4332 - 4346
反应条件
1.1: sulfuric acid / 80 - 90 °C 2.1: sulfuric acid; water 3.1: hydrazine hydrate / ethanol / Reflux 3.2: Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 24 p. 7349 - 7353
反应条件
1: With sulfuric acid T=60 - 80°C; 2: With water 0.5 h; Cooling with ice;
参考文献
Wang, Lihong; Li, Zhanshan; Lu, Lianhong; Zhang, Wei
Tetrahedron, 2012 , vol. 68, # 5 p. 1483 - 1491
参考文献
Piozzi; Favini
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1955 , vol. <8>18, p. 647,653
反应条件
T=60 - 75°C; Behandeln des Reaktionsproduktes mit Wasser;
参考文献
Sandmeyer
Helvetica Chimica Acta, 1919 , vol. 2, p. 239
Full Text Show Details
Geigy A.-G.
Patent: DE313725 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 13, p. 448
反应条件
1: H2SO4 / 0.17 h / 80 °C
2: ethanol
View Scheme
参考文献
Biyala, Mukesh Kumar; Fahmi, Nighat; Singh
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2004 , vol. 43, # 12 p. 2536 - 2541
