4-苯基吡啶-N-氧化物合成路线 （共 20 条）
反应条件
bis(trimethylsilyl)-peroxide; rhenic(VII) acid in dichloromethane; water T=24°C; 17 h;
参考文献
Tetrahedron Letters, , vol. 39, # 8 p. 761 - 764
反应条件
water; potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether
参考文献
Synlett, , # 1 p. 45 - 48
反应条件
n-Pentyl nitrite in acetic acid Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 32, # 5 p. 1780 - 1789
反应条件
in acetonitrile MeN4Cl adding to the polarographic test soln. prepared from SnCl4*5H2O in acetonitrile containing a ligand in a molar ratio 2:1 and 1 M Pr4NClO4 as a supporting electrolyte under N2; detected polarographically;
参考文献
Polyhedron, , vol. 2, p. 479 - 484
反应条件
1: Ts2O / various solvent(s); CH2Cl2 / 0.25 h / 20 °C 2: TFA / various solvent(s); CH2Cl2 / 70 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 12 p. 4554 - 4557
反应条件
in chloroform Kinetics; Re-complex and 4-PhOC5H4NO in chloroform at 25°C; monitored by UV/VIS spectroscopy;
参考文献
Shan, Xiaopeng; Ellern, Arkady; Guzei, Ilia A.; Espenson, James H.
Inorganic Chemistry, 2004 , vol. 43, # 13 p. 3854 - 3862
反应条件
in chloroform Kinetics; byproducts: O(CH2CH2S)2, C5H4(C6H5)N; react. of Re complex with pyridine deriv.in CHCl3 at 25°C, UV monitored;
参考文献
Shah, Xiaopeng; Ellern, Arkady; Guzei, Ilia A.; Espenson, James H.
Inorganic Chemistry, 2003 , vol. 42, # 7 p. 2362 - 2367
反应条件
1: With acetic anhydride 48 h; Heating / reflux; 2: With sodium hydrogencarbonate in water; ethyl acetate 3: With potassium carbonate in methanol T=20°C; 1 h;
参考文献
Dales, Natalie; Fonarev, Julia; Fu, Jianmin; Hou, Duanjie; Kamboj, Rajender; Kodumuru, Vishnumurthy; Pokrovskaia, Natalia; Raina, Vandna; Sun, Shaoyi; Zhang, Zaihui
Patent: US2009/156615 A1, 2009 ;
Location in patent: Page/Page column 17 ;
US 20090156615 A1
反应条件
monochloromethanesulfonyl chloride T=90°C; 24 h;
参考文献
Wang, Ying; Espenson, James H.
Organic Letters, 2000 , vol. 2, # 22 p. 3525 - 3526
反应条件
in acetonitrile T=81°C; 4 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 44, # 2 p. 487 - 489
