3-乙氧基-4-甲氧基苯甲醛合成路线 （共 31 条）
反应条件
hydrogen bromide; acetic acid
参考文献
C.F.Boehringer and Soehne
Patent: CH171034 , 1933 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 21, p. 394
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C.F.Boehringer and Soehne
Patent: DE622966 , 1932 ;
参考文献
Szantay
Acta Chimica Academiae Scientiarum Hungaricae, 1957 , vol. 12, p. 83,85, 89
参考文献
C.F. Boehringer and Soehne
Patent: DE622966 , 1932 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 21, p. 394
反应条件
alkaline aqueous potassium permanganate solution
参考文献
Spaeth; Bernhauer
Chemische Berichte, 1925 , vol. 58, p. 203
反应条件
1: 66 percent / pyridine / 5 h / 20 °C
2: 62 percent / diborane / tetrahydrofuran / 2 h / Heating
View Scheme
参考文献
Wrobel, Jay; Jetter, James; Kao, Wenling; Rogers, John; Di, Li; Chi, Jamin; Perez, M. Claudia; Chen, Gi-Chung; Shen, Emily S.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 16 p. 5729 - 5741
反应条件
1: copper oxide-chromium oxide; ethanol / Hydrogenation
2: benzene; hexane; HCl / -10 °C
3: aqueous acetone
4: aqueous NaOH
View Scheme
参考文献
Manske; Ashford
Journal of the American Chemical Society, 1951 , vol. 73, p. 5144
反应条件
toluene-4-sulfonic acid; acetic acid
Erwaermen des Reaktionsprodukts mit aethanol. KOH;
参考文献
Boeeseken; Greup
Recueil des Travaux Chimiques des Pays-Bas, 1939 , vol. 58, p. 528,532, 535
反应条件
1: 96 percent / PPh3 / CH2Cl2 / 0.67 h / cooling
2: 99 percent / nBuLi / pentane; tetrahydrofuran / 3 h / -78 - 23 °C
View Scheme
参考文献
Rosiak, Anna; Frey, Wolfgang; Christoffers, Jens
European Journal of Organic Chemistry, 2006 , # 17 p. 4044 - 4054
反应条件
bromine; acetic acid
参考文献
Stermitz; Gillespie; Amoros; Romero; Larson; Earl; Ogg
Journal of Medicinal Chemistry, 1975 , vol. 18, # 7 p. 708 - 713
反应条件
hydroxylamine hydrochloride in acetonitrile
T=5 - 84°C; Product distribution / selectivity;
参考文献
CELGENE CORPORATION; SAINDANE, Manohar, T.; GE, Chuansheng
Patent: WO2010/30345 A2, 2010 ;
Location in patent: Page/Page column 10 ;
WO 2010/030345 A2
