1-溴-2,4,6-三甲氧基苯合成路线 （共 19 条）
反应条件
N-bromosuccinmide in tetrachloromethane 3 h; Heating;
参考文献
Mondal, Mukulesh; Puranik, Vedavati G.; Argade, Narshinha P.
Journal of Organic Chemistry, 2006 , vol. 71, # 13 p. 4992 - 4995
反应条件
silver carbonate; copper(ll) bromide; palladium dichloride in tetrahydrofuran T=110°C; 24 h;
参考文献
Peng, Xuefeng; Shao, Xiang-Feng; Liu, Zhong-Quan
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3079 - 3081
反应条件
dihydrogen peroxide; sodium bromide; ethyl orthosilicate; gamma-aminopropyltriethoxysilane in 1,4-dioxane; phosphate buffer 24 h;
参考文献
Bennett, Stephanie M.; Tang, Ying; McMaster, Danielle; Bright, Frank V.; Detty, Michael R.
Journal of Organic Chemistry, 2008 , vol. 73, # 17 p. 6849 - 6852
反应条件
perchloric acid; dihydrogen peroxide; potassium bromide; NH4VO3 in methanol; water 24 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 611 - 612
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide
参考文献
Canadian Journal of Chemistry, , vol. 61, p. 1045 - 1052
反应条件
1: diethyl ether / 0 °C / dann bei 20grad 2: alkaline solution; alcohol / dann in Wasser 3: bei der Vakuumdestillation View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 460, p. 23
反应条件
1: alkaline solution; alcohol / dann in Wasser 2: bei der Vakuumdestillation View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 460, p. 23
反应条件
bei der Destillation im Vakuum;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 460, p. 23
参考文献
Justus Liebigs Annalen der Chemie, , vol. 276, p. 343
Justus Liebigs Annalen der Chemie, , vol. 277, p. 308
反应条件
1: 1-bromo-2,4,6-trimethoxybenzene With n-butyllithium in tetrahydrofuran T=-78°C; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran T=-78 - 0°C; 0.75 h; Inert atmosphere; 3: benzyl chloride With PdCl2(DPEphos) in tetrahydrofuran T=0 - 70°C; Negishi coupling; Inert atmosphere;
参考文献
Dennis, Eric G.; Jeffery, David W.; Perkins, Michael V.; Smith, Paul A.
Tetrahedron, 2011 , vol. 67, # 11 p. 2125 - 2131
