3,5-二甲基-1-苯基吡唑合成路线 （共 43 条）
反应条件
in neat (no solvent) T=120°C; 0.0833333 h; Microwave irradiation;
参考文献
Vaddula, Buchi Reddy; Varma, Rajender S.; Leazer, John
Tetrahedron Letters, 2013 , vol. 54, # 12 p. 1538 - 1541
反应条件
caesium carbonate; copper(I) oxide in N,N-dimethyl-formamide T=110°C; 54 h;
参考文献
Taillefer, Marc; Cristau, Henri-Jean; Cellier, Pascal-Philippe
Patent: US2005/234239 A1, 2005 ;
Location in patent: Page/Page column 23; 26-27 ;
反应条件
potassium phosphate; 6-pyrazol-1-ylpyridine-3-carboxylic acid; copper(l) chloride in N,N-dimethyl-formamide T=100°C; 24 h; Inert atmosphere;
参考文献
Liu, Hai-Yang; Yu, Zhen-Tao; Yuan, Yong-Jun; Yu, Tao; Zou, Zhi-Gang
Tetrahedron, 2010 , vol. 66, # 47 p. 9141 - 9144
反应条件
Cu(II)(MeCOCHCO2Et)2 in water T=40°C; P=760.051 Torr; 96 h;
参考文献
Joubert, Nicolas; Basle, Emmanuel; Vaultier, Michel; Pucheault, Mathieu
Tetrahedron Letters, 2010 , vol. 51, # 22 p. 2994 - 2997
反应条件
toluene-4-sulfonic acid in ethanol T=80°C; 24 h; Inert atmosphere; Reagent/catalyst;
参考文献
Organic Letters, , vol. 16, # 2 p. 596 - 599
反应条件
acetic acid in ethanol T=20°C; 1 h;
参考文献
Alberola, Angel; Calvo Bleye, Luis; Gonzalez-Ortega, Alfonso; Sadaba, M.Luisa; Sanudo, M.Carme
Heterocycles, 2001 , vol. 55, # 2 p. 331 - 352
反应条件
1: With toluene-4-sulfonic acid in ethanol T=80°C; 24 h; Inert atmosphere; 2: in diethyl ether Inert atmosphere;
参考文献
Organic Letters, , vol. 16, # 2 p. 596 - 599
反应条件
1: chlorobenzene With t-Bu-BippyPhos; [Pd(η3-1-Ph-allyl)(μ-Cl)]2; hydrazine hydrate; sodium t-butanolate in toluene T=110°C; Buchwald-Hartwig Coupling; 1 h; Inert atmosphereGlovebox; 2: acetylacetone T=110°C; Buchwald-Hartwig Coupling; Inert atmosphereGlovebox;
参考文献
Crawford, Sarah M.; Lavery, Christopher B.; Stradiotto, Mark
Chemistry - A European Journal, 2013 , vol. 19, # 49 p. 16760 - 16771
反应条件
Cu-exchanged fluoroapatite; air in methanol T=20°C; 24 h;
参考文献
Kantam, Mannepalli Lakshmi; Venkanna, Gopaladasu Tirupati; Kumar, Kota Balaji Shiva; Subrahmanyam, Vura Bala
Helvetica Chimica Acta, 2010 , vol. 93, # 5 p. 974 - 979
反应条件
in ethanol 3 h; Reflux;
参考文献
Reddy, Cherkupally Sanjeeva; Kumar, Gaddam Rajesh; Devi, MacHerla Vani; Nagaraj, Adki
Acta Chimica Slovenica, 2011 , vol. 58, # 3 p. 576 - 581
