4-(1,1-二甲基乙基)-3,5-环己二烯-1,2-二酮合成路线 （共 24 条）
反应条件
1: 45 percent / 1 h / Ambient temperature; Irradiation 2: potassium carbonate / ethane-1,2-diol / 4 h / 120 °C 3: 1.) N-bromosuccinimide (NBS), AIBN, 2.) NaI / 1.) carbon tetrachloride, 12 h, reflux, 2.) acetone, 2 h, reflux View Scheme
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Journal of Organic Chemistry, 1987 , vol. 52, # 25 p. 5616 - 5621
反应条件
[bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane T=0 - 20°C; 2.5 h; Inert atmosphere;
参考文献
Nemoto, Hiroyuki; Nishiyama, Tsuyoshi; Akai, Shuji
Organic Letters, 2011 , vol. 13, # 10 p. 2714 - 2717
反应条件
in acetonitrile-D3 0.416667 h; other substituted benzoquinones; Mechanism;
参考文献
Mure, Minae; Klinman, Judith P.
Journal of the American Chemical Society, 1995 , vol. 117, # 34 p. 8698 - 8706
反应条件
NADH-H+ in water; acetonitrile T=30°C; pH=7.0; Rate constant;
参考文献
Lam; Garg; Swanson; Pezzuto
Journal of Pharmaceutical Sciences, 1988 , vol. 77, # 5 p. 393 - 395
反应条件
1 h; Ambient temperatureIrradiation;
参考文献
Journal of Organic Chemistry, , vol. 52, # 25 p. 5616 - 5621
反应条件
sodium hydroxide; sodium metasilicate; diethylenetriamine-N,N,N',N'',N''-pentaacetic acid; dihydrogen peroxide in water T=40°C; 1 h; pH 10.0; Mechanism;
参考文献
Gellerstedt, Goeran; Hardell, Hanne-Lise; Lindfors, Eva-Lisa
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 9 p. 669 - 674
反应条件
1 h; Ambient temperatureIrradiation;
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Journal of Organic Chemistry, 1987 , vol. 52, # 25 p. 5616 - 5621
反应条件
in benzene Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 11 p. 3657 - 3658
反应条件
in acetonitrile-D3 0.416667 h; other substituted benzoquinones; Mechanism;
参考文献
Journal of the American Chemical Society, , vol. 117, # 34 p. 8698 - 8706
反应条件
tert.-butylhydroperoxide; tris(triphenylphosphine)ruthenium(II) chloride in acetone
18 h; Ambient temperature;
参考文献
Barth, Michael; Shah, Syed Tasadaque Ali; Rademann, Joerg
Tetrahedron, 2004 , vol. 60, # 39 p. 8703 - 8709
