1: 2 h / 200 °C 2: 98 percent / boron trichloride / CH2Cl2 / 2 h / 0 °C 3: 1.) n-butyl-lithium, triphenylmethane, 2.) pyridine / multistep reaction; the various dehydrohalogenated products with other bases, without acetylation; other tertiary halides View Scheme
参考文献
Baird, Kenneth J.; Grundon, Michael F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1820 - 1825
1: 2 h / 200 °C
2: 98 percent / boron trichloride / CH2Cl2 / 2 h / 0 °C
3: n-butyl lithium / diethyl ether / 20 °C
View Scheme
参考文献
Baird, Kenneth J.; Grundon, Michael F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1820 - 1825
