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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
112533-27-4
合成路线
(共 5 条)
112533-31-0
→
反应条件
112533-27-4
反应条件
potassium dichromate; sulfuric acid T=55°C;
参考文献
Chow, Tahsin J.; Wu, Tung-Kung
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 1102 - 1103
17872-39-8
→
反应条件
119347-55-6
+
112533-27-4
反应条件
pyridine; pyridine-2-carboxylic acid; tert.-butylhydroperoxide; [iron(II)(H2O)6](perchlorate)2; oxygen; lithium chloride; ascorbic acid powder in water 120 h; Ambient temperaturefurther oxidizing agents; Further byproducts given;
参考文献
Marchand, Alan P.; Wang, Yanjun; Alihodzic, Sulejman; Barton, Derek H. R.
Tetrahedron, 1997 , vol. 53, # 4 p. 1257 - 1264
17872-39-8
→
反应条件
112533-27-4
+
112533-33-2
反应条件
pyridine; pyridine-2-carboxylic acid; tert.-butylhydroperoxide; [iron(II)(H2O)6](perchlorate)2; oxygen; lithium chloride; ascorbic acid powder in water 120 h; Ambient temperaturefurther oxidizing agents; Further byproducts given;
参考文献
Marchand, Alan P.; Wang, Yanjun; Alihodzic, Sulejman; Barton, Derek H. R.
Tetrahedron, 1997 , vol. 53, # 4 p. 1257 - 1264
110-86-1
吡啶
+
17872-39-8
→
反应条件
119347-55-6
+
112533-27-4
反应条件
pyridine-2-carboxylic acid; tert.-butylhydroperoxide; [iron(II)(H2O)6](perchlorate)2; oxygen; acetic acid; lithium chloride in water 120 h; Ambient temperaturefurther oxidizing agents; Further byproducts given;
参考文献
Marchand, Alan P.; Wang, Yanjun; Alihodzic, Sulejman; Barton, Derek H. R.
Tetrahedron, 1997 , vol. 53, # 4 p. 1257 - 1264
110-86-1
吡啶
+
17872-39-8
→
反应条件
112533-27-4
反应条件
pyridine-2-carboxylic acid; tert.-butylhydroperoxide; [iron(II)(H2O)6](perchlorate)2; oxygen; acetic acid; lithium chloride in water 120 h; Ambient temperaturefurther oxidizing agents; Further byproducts given;
参考文献
Marchand, Alan P.; Wang, Yanjun; Alihodzic, Sulejman; Barton, Derek H. R.
Tetrahedron, 1997 , vol. 53, # 4 p. 1257 - 1264