1: 99 percent / Jones reagent / acetone / Ambient temperature 2: oxalyl chloride / 2 h / Heating View Scheme
参考文献
Porter, Ned A.; Rosenstein, Ian J.; Breyer, Robert A.; Bruhnke, John D.; Wu, Wen-Xue; McPhail, Andrew T.
Journal of the American Chemical Society, 1992 , vol. 114, # 20 p. 7664 - 7676
1: With 1H-imidazole; triphenylphosphine in diethyl ether; acetonitrile 0.166667 h; cooling; 2: With iodine in diethyl ether; acetonitrile 1 h; cooling; Further stages.;
Porter, Ned A.; Rosenstein, Ian J.; Breyer, Robert A.; Bruhnke, John D.; Wu, Wen-Xue; McPhail, Andrew T.
Journal of the American Chemical Society, 1992 , vol. 114, # 20 p. 7664 - 7676