2,6-二(1-甲基苯并咪唑-2-基)吡啶合成路线 （共 6 条）
反应条件
1: bzimpy With sodium hydride in N,N-dimethyl-formamide T=35°C; 1 h; 2: methyl iodide in N,N-dimethyl-formamide T=40°C; 3 h;
参考文献
IDEMITSU KOSAN CO., LTD.; Chuo University
Patent: EP1816134 A1, 2007 ;
Location in patent: Page/Page column 27 ;
反应条件
polyphosphoric acid T=210°C; 4 h; Neat (no solvent);
参考文献
Yang, Wen-Wen; Zhong, Yu-Wu; Yoshikawa, Shinpei; Shao, Jiang-Yang; Masaoka, Shigeyuki; Sakai, Ken; Yao, Jiannian; Haga, Masa-Aki
Inorganic Chemistry, 2012 , vol. 51, # 2 p. 890 - 899
反应条件
potassium in tetrahydrofuran 1 h; Inert atmosphereReflux;
参考文献
Wu, Huilu; Huang, Xingcai; Yuan, Jingkun; Kou, Fan; Jia, Fei; Liu, Bin; Bai, Ying
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2011 , vol. 66, # 10 p. 1049 - 1055
参考文献
Addison, Anthony W.; Burman, Sudhir; Wahlgren, Curtis G.; Rajan, Odatt A.; Rowe, Teresa M.; Sinn, Ekkehard
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 2621 - 2630
反应条件
in dimethyl sulfoxide Conductometric titration.;
参考文献
Piguet, Claude; Bocquet, Bernard; Mueller, Edgar; Williams, Alan F.
Helvetica Chimica Acta, 1989 , vol. 72, p. 323 - 337
反应条件
in N,N-dimethyl-formamide Addn. of Et4NCl soln. to soln. of ligand.; Addn. of Et2O to precipitate the complex, filtn., washing (CH2Cl2), recrystn. (DMF/Et2O).;
参考文献
Piguet, Claude; Bocquet, Bernard; Mueller, Edgar; Williams, Alan F.
Helvetica Chimica Acta, 1989 , vol. 72, p. 323 - 337
