a-乙酰-a-甲基-γ-丁内酯合成路线 (共 11 条)
反应条件
1: 3-acetyltetrahydrofuran-2-one With sodium methylate in benzene 2: methyl iodide Further stages.;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 4 p. 379 - 389
反应条件
sodium hydride; N,N-dimethyl-formamide; benzene Erwaermen des Reaktionsgemisches mit Methyljodid;
参考文献
Journal of the American Chemical Society, , vol. 80, p. 6341,6345
反应条件
1: 78 percent / sodium hydroxide / H2O; ethanol / 50 h / -5 - 0 °C 2: 72 percent / sodium 2-metyhylbutan-2-olate / benzene / 24 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2585 - 2598
反应条件
sodium hydride in ethylene glycol dimethyl ether Yield given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 22 p. 2597 - 2598
反应条件
anschl. mit Methyljodid;
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 1042; engl. Ausg. S. 1124
反应条件
T=510.1°C; var. temp., Ea; Rate constantThermodynamic data;
参考文献
Al-Awadi, Nouria A.; Mathew, Tommy
International Journal of Chemical Kinetics, 1995 , vol. 27, # 9 p. 843 - 848
反应条件
sodium ethanolate in ethanol 5 h; Heating;
参考文献
Brun, Kathrin A.; Heimgartner, Heinz
Helvetica Chimica Acta, 2005 , vol. 88, # 11 p. 2951 - 2959
反应条件
T=510.1°C; var. temp., Ea; Rate constantThermodynamic data;
参考文献
Al-Awadi, Nouria A.; Mathew, Tommy
International Journal of Chemical Kinetics, 1995 , vol. 27, # 9 p. 843 - 848
反应条件
sodium iodide in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=180°C;
参考文献
Murakami, Masashi; Nishida, Shinya
Chemistry Letters, 1981 , p. 997 - 1000
反应条件
hydrogenchloride Heating;
参考文献
Allen, Paul R.; Brimble, Margaret A.; Prabaharan, Hishani
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 4 p. 379 - 389