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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
112290-59-2
合成路线
（共 9 条）
112290-59-2
+
107-13-1
丙烯腈
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
+
86563-27-1
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol T=30 - 35°C; 0.75 h; Irradiation; Further byproducts given;
参考文献
Praly, Jean-Pierre; Ardakani, Azin Salek; Bruyere, Isabelle; Marie-Luce, Chrystelle; Bing Qin, Bing
Carbohydrate Research, 2002 , vol. 337, # 18 p. 1623 - 1632
4851-64-3
二乙基乙烯基磷酸酯
+
112290-59-2
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
反应条件
1: With 2,2'-azo-bisisobutyronitrile; tributyltin chloride; n-Bu4NBH3CN in benzene 1.5 h; Irradiation; 2: With tri-n-butyl-tin hydride 0.5 h; Irradiation; Further byproducts given;
参考文献
Praly, Jean-Pierre; Ardakani, Azin Salek; Bruyere, Isabelle; Marie-Luce, Chrystelle; Bing Qin, Bing
Carbohydrate Research, 2002 , vol. 337, # 18 p. 1623 - 1632
112290-59-2
+
107-13-1
丙烯腈
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
+
144427-70-3
+
144427-69-0
+
144427-71-4
+
13137-69-4
+
4451-35-8
2,3,4,6-TETRA-O-ACETYL-ALPHA-D-GLUCOPYRANOSYL CHLORIDE
反应条件
tri-n-butyl-tin hydride in benzene HeatingIrradiationother solvents; Product distributionMechanism;
参考文献
Praly; El Kharraf; Descotes
Carbohydrate Research, 1992 , vol. 232, # 1 p. 117 - 123
112290-59-2
+
107-13-1
丙烯腈
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
+
86563-27-1
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol T=30 - 35°C; 0.75 h; Irradiation; Further byproducts given;
参考文献
Praly, Jean-Pierre; Ardakani, Azin Salek; Bruyere, Isabelle; Marie-Luce, Chrystelle; Bing Qin, Bing
Carbohydrate Research, 2002 , vol. 337, # 18 p. 1623 - 1632
4851-64-3
二乙基乙烯基磷酸酯
+
112290-59-2
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
反应条件
1: With 2,2'-azo-bisisobutyronitrile; tributyltin chloride; n-Bu4NBH3CN in benzene 1.5 h; Irradiation; 2: With tri-n-butyl-tin hydride 0.5 h; Irradiation; Further byproducts given;
参考文献
Praly, Jean-Pierre; Ardakani, Azin Salek; Bruyere, Isabelle; Marie-Luce, Chrystelle; Bing Qin, Bing
Carbohydrate Research, 2002 , vol. 337, # 18 p. 1623 - 1632
112290-59-2
+
107-13-1
丙烯腈
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
+
144427-70-3
+
144427-69-0
+
144427-71-4
+
13137-69-4
+
4451-35-8
2,3,4,6-TETRA-O-ACETYL-ALPHA-D-GLUCOPYRANOSYL CHLORIDE
反应条件
tri-n-butyl-tin hydride in benzene HeatingIrradiationother solvents; Product distributionMechanism;
参考文献
Praly; El Kharraf; Descotes
Carbohydrate Research, 1992 , vol. 232, # 1 p. 117 - 123
112290-59-2
+
107-13-1
丙烯腈
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
+
86563-27-1
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol T=30 - 35°C; 0.75 h; Irradiation; Further byproducts given;
参考文献
Carbohydrate Research, , vol. 337, # 18 p. 1623 - 1632
4851-64-3
二乙基乙烯基磷酸酯
+
112290-59-2
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
反应条件
1: With 2,2'-azo-bisisobutyronitrile; tributyltin chloride; n-Bu4NBH3CN in benzene 1.5 h; Irradiation; 2: With tri-n-butyl-tin hydride 0.5 h; Irradiation; Further byproducts given;
参考文献
Carbohydrate Research, , vol. 337, # 18 p. 1623 - 1632
112290-59-2
+
107-13-1
丙烯腈
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
+
144427-70-3
+
144427-69-0
+
144427-71-4
+
13137-69-4
+
4451-35-8
2,3,4,6-TETRA-O-ACETYL-ALPHA-D-GLUCOPYRANOSYL CHLORIDE
反应条件
tri-n-butyl-tin hydride in benzene HeatingIrradiationother solvents; Product distributionMechanism;
参考文献
Carbohydrate Research, , vol. 232, # 1 p. 117 - 123
