反应条件
Multi-step reaction with 4 steps 1: NaBH4 / ethanol / 1 h / -15 - -10 °C2: 80 percent / TsOH*H2O / 1.) r.t., 24 h, 2.) 50 deg C, 7 h3: 100 percent / 1 M aq. NaOH / ethanol / 18 h / Ambient temperature4: (COCl)2, DMF / toluene / 1 h
参考文献
Parkes, Kevin E. B.; Bushnell, David J.; Crackett, Peter H.; Dunsdon, Stephen J.; Freeman, Andrew C.; et al. Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3656 - 3664
