2-氟-1-(1-萘基)乙酮合成路线 （共 9 条）
反应条件
aluminium trichloride; ethanethiol in dichloromethane T=0°C; 0.333333 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1043 - 1048
反应条件
1: With methanol; accufluorTM in acetonitrile
Fluorination; Ketalization;
2: With hydrogenchloride in acetonitrile
Hydrolysis; Further stages.;
参考文献
Stavber, Stojan; Jereb, Marjan; Zupan, Marko
Chemical Communications, 2000 , # 14 p. 1323 - 1324
反应条件
hydrogenchloride
T=20°C;
参考文献
Surya Prakash; Hu; Olah
Journal of Fluorine Chemistry, 2001 , vol. 112, # 2 p. 357 - 362
反应条件
1: Mg / tetrahydrofuran / 2 h / 0 °C
2: aq. HCl / 20 °C
View Scheme
参考文献
Surya Prakash; Hu; Olah
Journal of Fluorine Chemistry, 2001 , vol. 112, # 2 p. 357 - 362
反应条件
1: Mg / tetrahydrofuran / 2 h / 0 °C
2: aq. HCl / 20 °C
3: Mg / tetrahydrofuran / 2 h / 0 °C
4: aq. HCl / 20 °C
View Scheme
参考文献
Surya Prakash; Hu; Olah
Journal of Fluorine Chemistry, 2001 , vol. 112, # 2 p. 357 - 362
反应条件
1: aq. HCl / 20 °C
2: Mg / tetrahydrofuran / 2 h / 0 °C
3: aq. HCl / 20 °C
View Scheme
参考文献
Surya Prakash; Hu; Olah
Journal of Fluorine Chemistry, 2001 , vol. 112, # 2 p. 357 - 362
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate)
参考文献
Fuglseth, Erik; Otterholt, Eli; Hogmoen, Hanne; Sundby, Eirik; Charnock, Colin; Hoff, Bard Helge
Tetrahedron, 2009 , vol. 65, # 47 p. 9807 - 9813
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate)
1 h; Microwave irradiation;
参考文献
Krane Thvedt, Thor Hakon; Fuglseth, Erik; Sundby, Eirik; Hoff, Bard Helge
Tetrahedron, 2009 , vol. 65, # 46 p. 9550 - 9556
参考文献
Fuji, Kaoru; Node, Manabu; Kawabata, Takeo; Fujimoto, Mayumi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1043 - 1048
