6-甲基-2-吡啶基甲醇合成路线 (共 23 条)
反应条件
sodium tetrahydroborate in ethanol T=0°C;
参考文献
Feig, Andrew L.; Lippard, Stephen J.
Journal of the American Chemical Society, 1994 , vol. 116, # 18 p. 8410 - 8411
参考文献
Yakugaku Zasshi, , vol. 74, p. 790
Chem.Abstr., , p. 11646
Helvetica Chimica Acta, , vol. 38, p. 1114,1116
Yakugaku Zasshi, , vol. 78, p. 661,665
Chem.Abstr., , p. 18399
反应条件
sulfuric acid in water T=95°C; 5 h;
参考文献
Jones, Gurnos; Mouat, Deborah J.; Tonkinson, Daryl J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2719 - 2724
反应条件
hydrogenchloride in methanol; dichloromethane
参考文献
US6255305 B1, ;
US 6255305 B1
反应条件
trifluoroacetic anhydride in N,N-dimethyl-formamide 16 h; Ambient temperature;
参考文献
Konno, Katsuhiro; Hashimoto, Kimiko; Shirahama, Haruhisa; Matsumoto, Takeshi
Heterocycles, 1986 , vol. 24, # 8 p. 2169 - 2172
反应条件
cis-IrCl(CO)(PPh3)2; hydrazine hydrate; potassium hydroxide in methanol T=160°C; Wolff-Kishner Reduction; 3 h; Sealed tube;
参考文献
European Journal of Organic Chemistry, , # 29 p. 6496 - 6500
反应条件
1: CH2Cl2 / 1.5 h / Ambient temperature 2: aq. (NH4)2S2O8 / 1 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 19, # 1, 2 p. 317 - 326
反应条件
Ba(OH)2 monohydrate in ethanol Claisen-Schmidt Condensation; 0.75 h; Reflux;
参考文献
Tetrahedron Letters, , vol. 53, # 42 p. 5660 - 5662
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the Chemical Society, , p. 3594,3601
反应条件
(NH4)2S2O8 1 h; Heating; Yield given. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 19, # 1, 2 p. 317 - 326