7-溴双环[4.1.0]庚烷合成路线 （共 22 条）
反应条件
sodium dithionite; sodium hydrogencarbonate in N,N-dimethyl-formamide; isopropyl alcohol
2.5 h; Heating;
参考文献
D'yachenko, A. I.; Korneva, O. S.; Abramova, N. M.; Nefedov, O. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 12 p. 2583 - 2584
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 12 p. 2818 - 2820
反应条件
lithium aluminium tetrahydride; silver perchlorate in tetrahydrofuran
T=-20°C; 0.25 h;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Chemistry Letters, 1983 , p. 1877 - 1878
反应条件
magnesium chloride in tetrahydrofuran
T=-50 - -40°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Ando, Teiichi; Muranaka, Takeshi; Ishihara, Takashi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3227 - 3228
反应条件
magnesium chloride in tetrahydrofuran
T=-50 - -40°C; 8 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Ando, Teiichi; Muranaka, Takeshi; Ishihara, Takashi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3227 - 3228
反应条件
chromium hexacarbonyl in dimethyl sulfoxide
T=130°C; Inert atmosphere;
参考文献
Lin, Shaw-Tao; Lee, Chuan-Chen; Ding, Mei-Fang; Liang, David W.; Jeng, An-Ting
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 529 - 534
反应条件
magnesium chloride in tetrahydrofuran
T=-50 - -40°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Ando, Teiichi; Muranaka, Takeshi; Ishihara, Takashi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3227 - 3228
反应条件
magnesium chloride in tetrahydrofuran
T=-50 - -40°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Ando, Teiichi; Muranaka, Takeshi; Ishihara, Takashi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3227 - 3228
反应条件
magnesium chloride in tetrahydrofuran
T=-50 - -40°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Ando, Teiichi; Muranaka, Takeshi; Ishihara, Takashi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 10 p. 3227 - 3228
反应条件
1: in tetrahydrofuran
T=20°C; 24 h;
2: With water in tetrahydrofuran
T=20°C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Baird, Mark S; Nizovtsev, Alexey V; Bolesov, Ivan G
Tetrahedron, 2002 , vol. 58, # 8 p. 1581 - 1593
反应条件
1: in tetrahydrofuran
T=20°C; 24 h;
2: With water-d2 in tetrahydrofuran
T=20°C; Further byproducts given. Title compound not separated from byproducts;
参考文献
Baird, Mark S; Nizovtsev, Alexey V; Bolesov, Ivan G
Tetrahedron, 2002 , vol. 58, # 8 p. 1581 - 1593
