2-(1-三氟甲基-2-硝基乙基)环己酮合成路线 (共 3 条)
反应条件
in dichloromethane T=20°C; Michael reaction; 2 h;
参考文献
Molteni, Marco; Consonni, Roberto; Giovenzana, Tommaso; Malpezzi, Luciana; Zanda, Matteo
Journal of Fluorine Chemistry, 2006 , vol. 127, # 7 p. 901 - 908
反应条件
1: 85 percent / benzene / 3 h 2: 71 percent / aq. sulfuric acid / 3 h View Scheme
参考文献
Aizikovich, A. Ya.; Korotaev, V. Yu.; Yaroslavtseva, L. E.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 7.1 p. 1045 - 1047
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 7 p. 989 - 991
反应条件
hydrogenchloride 1.) benzene, 20 min, 2.) 1 h; Yield given. Multistep reaction;
参考文献
Aizikovich, A. Ya.; Bazyl', I. T.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1203 - 1204
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1330 - 1332