(S)-2-噁丙环乙酸乙酯合成路线 (共 9 条)
反应条件
Jacobsen's (S,S)-(salen)Co(III) catalyst; air; acetic acid in tetrahydrofuran T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
Jacobsen's (S,S)-(salen)Co(III) catalyst; air; acetic acid in tetrahydrofuran T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
silver(l) oxide in acetonitrile Ambient temperature;
参考文献
Huang, Guangfei; Hollingsworth, Rawle I.
Tetrahedron Asymmetry, 1998 , vol. 9, # 23 p. 4113 - 4115
反应条件
water; acetic acid optical yield given as percent ee;
参考文献
Cui, Yubo; Tu, Wangyang; Floreancig, Paul E.
Tetrahedron, 2010 , vol. 66, # 26 p. 4867 - 4873
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Larcheveque; Henrot
Tetrahedron, 1990 , vol. 46, # 12 p. 4277 - 4282
反应条件
FAS; mercury(II) dithiocyanate in ethanol T=30°C; pH=7.5; Enzymatic reaction; Kinetics;
参考文献
ChemBioChem, , vol. 14, # 7 p. 870 - 881
反应条件
copper(l) iodide 1.) THF, -30 deg C, 30 min, 2.) THF, a) -30 deg C, 1 h, b) RT, overnight; Yield givenMultistep reaction;
参考文献
Huang, Guangfei; Hollingsworth, Rawle I.
Tetrahedron Asymmetry, 1998 , vol. 9, # 23 p. 4113 - 4115
反应条件
ammonia; nickel dichloride in aq. phosphate buffer; water T=30°C; pH=8; Enzymatic reaction; Kinetics;
参考文献
Schallmey, Marcus; Floor, Robert J.; Hauer, Bernhard; Breuer, Michael; Jekel, Peter A.; Wijma, Hein J.; Dijkstra, Bauke W.; Janssen, Dick B.
ChemBioChem, 2013 , vol. 14, # 7 p. 870 - 881
反应条件
in tetrahydrofuran; diethyl ether T=-30°C; 1 h;
参考文献
Larcheveque, Marc; Henrot, Serge
Tetrahedron Letters, 1987 , vol. 28, # 16 p. 1781 - 1782