1: 1-bromo-butane With iodine; magnesium in diethyl ether T=60°C; 1 h; 2: 1-bromo-decane With 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; ferrous acetate in diethyl ether T=20°C; Kumada coupling reaction; 0.25 h; Further stages. Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1015 - 1018
1: With magnesium in tetrahydrofuran Grignard Reaction; Inert atmosphereReflux; 2: With dilithium tetrachlorocuprate(II); oxygen in tetrahydrofuran T=20°C; 2 h;
