1: With [CpFe(IMes)(CO)2]I; phenyl silane in tetrahydrofuran T=70°C; 1 h; Inert atmosphereIrradiation; 2: With methanol; sodium hydroxide in tetrahydrofuran; water T=20°C; 1 h; Inert atmosphere;
hydrogen; sodium methylate; homogeneous ruthenium complex in tetrahydrofuran T=100°C; P=37503.8 Torr; 2.5 h; Title compound not separated from byproducts.;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 39 p. 7473 - 7476
hydrogen; sodium methylate; homogeneous ruthenium complex in tetrahydrofuran T=100°C; P=37503.8 Torr; 2.5 h; Title compound not separated from byproducts.;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 39 p. 7473 - 7476
