sodium hydrogencarbonate in ethanol; water
Inert atmosphereRefluxLarge scale reaction;
参考文献
Zacharie, Boulos; Ezzitouni, Abdallah; Duceppe, Jean-Simon; Penney, Christopher
Organic Process Research and Development, 2009 , vol. 13, # 3 p. 581 - 583
1: SOCl2 / Ambient temperature
2: pyridine, 30percent H2O2 / diethyl ether / 1 h / Ambient temperature
View Scheme
参考文献
McBride, J. Michael; Bertman, Steven B.; Cioffi, Donna Z.; Segmuller, Brigitte E.; Weber, Bruce A.
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 161, p. 1 - 24