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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
111836-07-8
合成路线
（共 5 条）
111836-07-8
→
反应条件
145513-90-2
(2S,3aR,7aR)-八氢-1H-吲哚鎓-2-羧酸酯
反应条件
1: 97 percent / K2CO3 / acetone / 48 h / Ambient temperature 2: 90 percent / 2N NaOH / dimethylformamide / 48 h / Ambient temperature 4: tetrahydrofuran / 0.5 h / Ambient temperature; Irradiation 5: Raney nickel 6: 6N HCl View Scheme
参考文献
Barton, Derek H. R.; Guilhem, Jean; Herve, Yolande; Potier, Pierre; Thierry, Josiane
Tetrahedron Letters, 1987 , vol. 28, # 13 p. 1413 - 1416
111836-07-8
→
反应条件
80875-98-5
(2S,3aS,7aS)-八氢吲哚-2-羧酸
反应条件
1: 97 percent / K2CO3 / acetone / 48 h / Ambient temperature 2: 90 percent / 2N NaOH / dimethylformamide / 48 h / Ambient temperature 4: tetrahydrofuran / 0.5 h / Ambient temperature; Irradiation 5: Raney nickel 6: 6N HCl View Scheme
参考文献
Barton, Derek H. R.; Guilhem, Jean; Herve, Yolande; Potier, Pierre; Thierry, Josiane
Tetrahedron Letters, 1987 , vol. 28, # 13 p. 1413 - 1416
111836-07-8
→
反应条件
108507-45-5
反应条件
Multi-step reaction with 6 steps 1: 81 percent / K2CO3 / acetone / Ambient temperature2: 92 percent / 2N NaOH / dimethylformamide / Ambient temperature4: tetrahydrofuran / 0.5 h / Ambient temperature; Irradiation5: Raney nickel / ethanol / Ambient temperature6: trifluoroacetic acid / 1 h / Ambient temperature
参考文献
Barton, Derek H. R.; Guilhem, Jean; Herve, Yolande; Potier, Pierre; Thierry, Josiane Tetrahedron Letters, 1987 , vol. 28, # 13 p. 1413 - 1416
111836-07-8
→
反应条件
111836-10-3
反应条件
Multi-step reaction with 2 steps 1: 97 percent / K2CO3 / acetone / 48 h / Ambient temperature2: 90 percent / 2N NaOH / dimethylformamide / 48 h / Ambient temperature
参考文献
Barton, Derek H. R.; Guilhem, Jean; Herve, Yolande; Potier, Pierre; Thierry, Josiane Tetrahedron Letters, 1987 , vol. 28, # 13 p. 1413 - 1416
111836-07-8
→
反应条件
111836-12-5
反应条件
Multi-step reaction with 4 steps 1: 97 percent / K2CO3 / acetone / 48 h / Ambient temperature2: 90 percent / 2N NaOH / dimethylformamide / 48 h / Ambient temperature4: tetrahydrofuran / 0.5 h / Ambient temperature; Irradiation
参考文献
Barton, Derek H. R.; Guilhem, Jean; Herve, Yolande; Potier, Pierre; Thierry, Josiane Tetrahedron Letters, 1987 , vol. 28, # 13 p. 1413 - 1416
