反应条件
in neat (no solvent)
under N2; Al-compd. added slowly over a period of 2 h to Sb-compd. at 0°C with stirring, warmed slowly to room temp., stirred for 4 h, heated for 12 h at 120°C;; monitored by NMR, fractional distn., Al-compd. isolated by distn.;;
参考文献
Thomas, C. J.; Krannich, L. K.; Watkins, C. L.
Polyhedron, 1993 , vol. 12, p. 89 - 94
