反应条件
in neat (no solvent) byproducts: (CH3)2Si(OCH3)Cl; to a freshly distd. PCl3 at 20°C silane is dropwise added, 10-25 min, ratio PCl3:silane=1:3; chlorosilane is distd. off;
参考文献
Krolevets, A. A.; Antipova, V. V.; Martynov, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 12 p. 2483 - 2485
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 12 p. 2847 - 2849