3-甲基-1,4-戊二烯合成路线 (共 15 条)
反应条件
DpSc-H T=80°C; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 110, # 3 p. 976 - 978
反应条件
(i) K, Et3N, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Yasuda,H. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 2036 - 2045
反应条件
1: n-butyllithium; 3-Methyl-1,4-pentadiene With potassium tert-butylate in tetrahydrofuran; hexane
T=0°C; 0.333333 h;
2: (MeO)2BF in tetrahydrofuran; hexane
T=-75°C;
3: With dihydrogen peroxide
Alkaline hydrolysis;
参考文献
Schlosser; Zellner; Leroux
Synthesis, 2001 , # 12 p. 1830 - 1836
反应条件
pyrolisis at various temperatures and pressures; Product distribution;
参考文献
Trenwith, Antony B.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1982 , vol. 78, p. 3131 - 3136
反应条件
(i) K, Et3N, (ii) H2O; Multistep reaction;
参考文献
Yasuda,H. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 2036 - 2045