NiCl2(PnBu3)2; diisobutyl-aluminum chloride in 1,1,2,2-tetrachloroethylene P=5481.8 Torr;

T=350°C; P=129287 Torr;

T=350°C; P=129287 Torr;

(i) K, Et3N, THF, (ii) /BRN= 969135/; Multistep reaction;

T=150°C; P=50 Torr; 6 h; Irradiationvarious temp. and pressure; Quantum yieldMechanism;

T=150°C; P=50 Torr; 6 h; Irradiationvarious temp. and pressure; Quantum yieldMechanism;

in dichloromethane T=20°C; Kinetics; Further Variations:Temperaturesconcentrations;

pyrolisis at various temperatures and pressures; Product distribution;

DpSc-H T=80°C; Product distribution;

1.1: hexane / 0 °C 1.2: 84 percent / tetrahydrofuran; hexane / -75 - 25 °C 2.1: 81 percent / triethyl(methoxycarbonylsulfamoyl)ammonium hydroxide / tetrahydrofuran / 0.25 h / 25 °C 3.1: LDA; NMPA / tetrahydrofuran; hexane 3.2: fluoromethoxyborane diethyl etherate; H2O2 (30percent); NaOH (3.0 M) / tetrahydrofuran / 2 h / 25 °C 3.3: 41 percent / pyridine / CH2Cl2 / 3 h / 25 °C View Scheme