potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate in toluene 18 h; Heating;

P(MeNCH2CH2)3N in hexane; acetonitrile T=0°C; 0.5 h;

暂无反应条件数据

benzene

ethanol; sodium ethanolate

1: 94 percent / LDA / tetrahydrofuran; hexane / 1 h / from 0 deg C to RT 2: 82 percent / TsOH / benzene / Heating 3: 80 percent / 50percent H2SO4/H2O, silica gel / CH2Cl2 / 2 h / Ambient temperature 4: 70 percent / NaBH4 / ethanol / 2 h / 0 °C 5: 73 percent / aq. H2SO4/silica gel / CH2Cl2 / 6 h / Ambient temperature 6: 70 percent / K2CO3 / acetone / 12 h / Heating 7: NaCl / dimethylsulfoxide / 160 °C View Scheme

暂无反应条件数据

sodium hydroxide

sodium hydroxide Erhitzen des Reaktionsprodukts mit wss. Schwefelsaeure;

Kochen;