1: trans vinyl bromide With magnesium in tetrahydrofuran Metallation; 2: 6,10,14-trimethyl-5,9,13-pentadecatrien-2-one in tetrahydrofuran T=0 - 20°C; Grignard reaction; 14 h;
参考文献
Odinokov; Akhmetova; Savchenko; Mallyabaeva; Lobanova
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 8 p. 1099 - 1101
1: 81 percent / DMAP / CH2Cl2 / 22 h / 0 - 20 °C 2: 80 percent / PdCl2(CH3CN)2 / tetrahydrofuran / 40 h 3: K2CO3 / methanol / 20 °C View Scheme
参考文献
Vlad, P. F.; Ungur, N. D.; Nguen Van Hung; Perutsky, V. B.
Russian Chemical Bulletin, 1995 , vol. 44, # 12 p. 2391 - 2403
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1995 , # 12 p. 2494 - 2506
