二甲基(3-氧代环戊基)丙二酸酯合成路线 (共 7 条)
反应条件
calcined Mg-Al-layered double hydroxide-supported iPr2-amide in methanol T=20°C; Michael addition; 24 h;
参考文献
Kantam, M. Lakshmi; Ravindra; Reddy, Ch. Venkat; Sreedhar; Choudary
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 4-5 p. 569 - 578
反应条件
benzophenone 10 h; Irradiation; Further byproducts given;
参考文献
L'Esperance, Robert P.; Ford, Thomas M.; Jones, Maitland
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 209 - 213
反应条件
in various solvent(s) 10 h; Irradiation; Further byproducts given;
参考文献
L'Esperance, Robert P.; Ford, Thomas M.; Jones, Maitland
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 209 - 213
反应条件
10 h; Irradiation; Further byproducts given;
参考文献
L'Esperance, Robert P.; Ford, Thomas M.; Jones, Maitland
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 209 - 213
反应条件
10 h; Irradiationreaction in the presence of benzophenone; Product distribution;
参考文献
L'Esperance, Robert P.; Ford, Thomas M.; Jones, Maitland
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 209 - 213
反应条件
1: toluene-4-sulfonic acid / toluene / 18 h / Reflux
2: sodium chloride / dimethyl sulfoxide / 3 h / 145 °C
View Scheme
参考文献
Puppala, Manohar; Murali, Annamalai; Baskaran, Sundarababu
Chemical Communications, 2012 , vol. 48, # 46 p. 5778 - 5780
反应条件
1: toluene-4-sulfonic acid / toluene / 18 h / Reflux
2: sodium chloride / dimethyl sulfoxide / 3 h / 145 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C
View Scheme
参考文献
Puppala, Manohar; Murali, Annamalai; Baskaran, Sundarababu
Chemical Communications, 2012 , vol. 48, # 46 p. 5778 - 5780