Na in neat (no solvent)
heating of (C2H5)3SiBr and Na at 140-145°C in a closed vessel;;
参考文献
Kraus, C. A.; Nilson, W. K.
Journal of the American Chemical Society, 1934 , vol. 56, p. 195 - 202
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Gmelin Handbook: Si: MVol.C, 114, page 320 - 323
(i) EtMgBr, (ii) /BRN= 1732870/; Multistep reaction;
参考文献
Shchukovwskaya,L.L.; Pal'chik,R.I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1964 , p. 2129 - 2131
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1964 , p. 2228 - 2230