3-氯-3-甲基-1-丁炔合成路线 (共 173 条)
反应条件
copper; calcium chloride; copper dichloride; hydrogenchloride T=0°C; 1 h;
参考文献
Stulgies, Balder; Prinz, Peter; Magull, Joerg; Rauch, Karsten; Meindl, Kathrin; Ruehl, Stephan; De Meijere, Armin
Chemistry - A European Journal, 2005 , vol. 11, # 1 p. 308 - 320
反应条件
thionyl chloride; 1,5-diethoxy-3-oxapentane
参考文献
Journal of the American Chemical Society, , vol. 82, p. 4094 - 4097
反应条件
3,4-dihydroxy-1-tert-butylbenzene; ammonium chloride; copper(l) chloride; phosphorus trichoride
参考文献
Journal of the American Chemical Society, , vol. 73, p. 4013
反应条件
hydrogenchloride 24 h; Ambient temperature;
参考文献
Stammann, Guenter; Griesbaum, Karl
Chemische Berichte, 1980 , vol. 113, # 2 p. 598 - 606
反应条件
hydrogenchloride 264 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 113, # 2 p. 598 - 606
反应条件
in diethyl ether; chloroform-d1 T=20°C; 336 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1845 - 1854
反应条件
hydrogenchloride T=26°C; 72 h; variat. of the rk.-time and the conc. of HCl; Product distributionMechanism;
参考文献
Chemische Berichte, , vol. 113, # 10 p. 3103 - 3111
参考文献
Journal of Biological Chemistry, , vol. 175, p. 801
Journal of the American Chemical Society, , vol. 70, p. 2855
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 200, p. 839
Zhurnal Obshchei Khimii, , vol. 9, p. 388
Chem. Zentralbl., , vol. 111, # I p. 526
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in toluene T=50°C; 88 h; MechanismProduct distribution;
参考文献
Reisch, Johannes; Bathe, Andreas; Salehi-Artimani, Reza A.
Archiv der Pharmazie (Weinheim, Germany), 1986 , vol. 319, # 8 p. 720 - 727