反应条件
catalyst: azobisisobutyronitrile in neat (no solvent) byproducts: MeSiCl3; boiling mixt. of MeGeCl3, MeSiHCl2 and catalyst (3 h), products quick driving off (vac.) into trap (solid CO2), MeSiCl3 and excess MeHSiCl2 sepn. by redistn., allyl chloride add. to residue, boiling 3 h, cooling.; vac. fraction distn., refractionation;
参考文献
Gar, T. K.; Khromova, N. Yu.; Tandura, S. N.; Nosova, V. M.; Kisin, A. V.; Mironov, V. F.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 545 - 550
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 622 - 628
