反应条件
pyridine; n-butyllithium; methyl iodide
1.) THF, hexane, -78 deg C, 30 min, 2.) -78 deg C, 2 h; -78 deg C -> 0 deg C, 3.) acetone, room temperature, 16 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Johnson,C.R.; Elliott,R.C.
Journal of the American Chemical Society, 1982 , vol. 104, p. 7041