反应条件
dihydrogen peroxide in water
K2Cr2O7 soln. and 30 percent H2O2 was added dropwise to stirred, cooled soln. of diethylenetriamine at 5°C over a period of 3 h; soln. kept at 2°C for 10 h, pale green crystals sepd., washed with EtOH and dried in vac.;
参考文献
Ranganathan, C. K.; Ramasami, T.; Ramaswamy, D.; Santappa, M.
Inorganic Chemistry, 1989 , vol. 28, p. 1306 - 1310
